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Die Kristallstruktur von [(THF)LiCl]n

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Die Kristallstruktur von [(THF)LiCl]

n

The Crystal Structure of [(THF)LiCl]

n

Mike R.Kopp and Bernhard Neumüller*

Fachbereich Chemie der Universität Marburg, Hans-Meerwein-Straße, D-35032 Marburg, Germany

Z.Naturforsch.54 b,818Ð820 (1999);

eingegangen am 27.Januar 1999

Lithiumchloride THF Solvate, Crystal Structure Single crystals of [(THF)LiCl]n (1) were ob- tained by the reaction of (PhCH2)2GaCl with LiSetBu in THF/toluene.1is polymeric in the so- lid state and crystallizes in the space group Pbcn, Z= 8, lattice dimensions atÐ83∞C:a= 1438.6(2), b= 1140.9(2),c= 746.2(1) pm,R1= 0.0395.

* Sonderdruckanforderungen an Priv.-Doz. Dr. B. Neumüller. Fax: +49 6421 288917.

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