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AB L

x L

y

2L

z

2sin L

k

: (6.15)

The transitionbetween both structures occurs, if F =0,resultingin

L

z

L

k

=

4sin

: (6.16)

ThecrossoverregimebetweenthetwostructuresintheL

z {L

k

diagramisbetweenthetwolines

with slope1=4 (for !0) and slope=8(for !=2). Bothlines are marked ing. 6.12 for

comparison, showing agreement with the simulations.

This result is also conrmed by experiments of an AC demixing process in thin lms on

an ABC{triblock copolymer brush, cf. the experiments of Fukunaga et al. [Fuk00] described

in sec. 1.4. The dierent geometry in the experiment yields only a dierent constant in the

righthandsideofeq.(6.16). Moreover,intheexperimentthesubstrateitselfconsistsofpolymer

block of type A and type B, therefore eectively only one interfacial tension

AB

has to be

considered and the ratio L

z

=L

k

can be determined directly.

4 6 10 8 20 30 40 50

6 8 10 20 30 40 50

L z

L ||

partial structure

full structure

Figure 6.12: Regions inthe L

z {L

k

plane, where the domainpattern inthe slab is fully structured

() and only partially structured (), in double logarithmic representation. The dividing lines are

given by the two limiting cases of eq. (6.16), L

z

= 1=4L

k

(straight line) and L

z

= =8L

k

(dashed

line).

6.4.2 Pattern Directed Spinodal Decomposition

In thissection weconsider thekinetics ofasystem similartothe onedescribed inthe previous

section, but for xed fraction f

A

=0:5. The initialconditions are asin sec. 6.3.3.

The intermediate scattering function

I

y (k

y

;z;t)= Z

1

0 dk

x I

k (k

k

;z;t); (6.17)

with I

k (k

k

;z;t) given in eq. (6.10) characterizes the domain formation with respect to the

pattern{direction.

t = 1000 MCS (a)

0 0.1 0.2 k y 0.3 0.4 0.5 0.6 0

1 2 3 4 5 6

z

1.0 10 -3 2.0 10 -3 3.0 10 -3

I y (k y ,z)

t = 10000 MCS (b)

0 0.1 0.2 k y 0.3 0.4 0.5 0.6 0

1 2 3 4 5 6

z

1.0 10 -3 2.0 10 -3 3.0 10 -3 4.0 10 -3

I y (k y ,z)

Figure 6.13: Intermediate scattering function I

y (k

y

;z;t) for a system of L

k

= 25 and L

z

= 6 at

times (a) t= 1000 MCS and (b) t =10000 MCS. The patterned structure is stable throughout the

whole lm.

The situation corresponding to a full structure in equilibrium is given in g. 6.13, where

I

y (k

y

;z;t) is shown for a thin slab of thickness L

z

= 6 and pattern periodicity L

k

= 25,

at two times. At early times (t = 1000 MCS, see g. 6.13a), a dominant structure arises

near the patterned substrate on the length scale k 1

y

= L

k

=2. This structure propagates in

z{direction until it reaches the opposite wall (t =10000 MCS, see g. 6.13b). At later times,

this structure is stable, as one would expect from g. 6.12. We determined no further change

inI

y (k

y

;z;t) untilt =30000 MCS.

Figure 6.14 shows I

y (k

y

;z;t) for a lm of thickness L

z

= 25 and pattern periodicity

L

k

= 12:5. This case corresponds to a partial structure in equilibrium. The pattern{induced

demixing is much faster than the lateral spinodaldecomposition. The pattern{induced

struc-t = 1000 MCS (a)

0 0.2 0.4 k y 0.6 0.8 1 1.2 0

5 10 15 20 25

z

2.0 10 -5 4.0 10 -5 6.0 10 -5 8.0 10 -5

I y (k y ,z)

t = 30000 MCS (b)

0 0.2 0.4 k y 0.6 0.8 1 1.2 0

5 10 15 20 25

z

2.0 10 -5 4.0 10 -5 6.0 10 -5

I y (k y ,z)

Figure 6.14: Intermediate scattering function I

y (k

y

;z;t) fora system ofL

k

=12:5 and L

z

=25 at

times (a) t= 1000 MCS and (b) t =30000 MCS. Lateral domaincoarsening occurs away from the

vicinityof thepatterned wall. Near thewallthestructure changes onlyweakly.

(a)

L || = 6

0 0.3 0.6 k y 0.9 1.2 1.5 0

2.5 5 7.5 10 12.5

z

1.0 10 -5 2.0 10 -5 3.0 10 -5 4.0 10 -5 5.0 10 -5

I y (k y ,z,t)

(b)

L || = 12.5

0 0.2

0.4 0.6

k y 0.8 0

2.5 5 7.5 10 12.5

z

1.0 10 -4 2.0 10 -4 3.0 10 -4 4.0 10 -4

I y (k y ,z,t)

(c)

L || = 25

0 0.2

0.4 0.6

k y 0.8 0

2.5 5 7.5 10 12.5

z

1.0 10 -4 2.0 10 -4 3.0 10 -4 4.0 10 -4 5.0 10 -4

I y (k y ,z,t)

Figure 6.15: Intermediate scattering function I

y (k

y

;z;t) for early demixing times t = 1000 MCS

and lmthicknessL

z

=12:5. The patternperiodicityis(a) L

k

=6,(b)L

k

=12:5 and (c)L

k

=25.

0 0.5 1 1.5

0 5 10 15 20 25

I y (2 π /L || , z, t) [10 -4 ]

z

50000 MCS 30000 MCS 10000 MCS 3000 MCS 1000 MCS

Figure6.16: IntermediatescatteringfunctionI

y (2=L

k

;z;t)asafunctionoftime. Thelmthickness

isL

z

=25and thepattern periodicityL

k

=50.

ture for small values of z leads to a much larger corresponding peak in I

y (k

y

;z;t), g. 6.14a,

than the disordered lateral domainpattern emerging for larger z. The ordered periodic

struc-ture propagates intothe lmover a nitedistance only(z 6,see g. 6.14b). For latertimes

(t=30000 MCS), the amplitude of the lateral decomposition waves is comparableto the

am-plitudeofthepattern{inducedwaves. However, the peakinI

y (k

y

;z;t)occursatsmallervalues

of k

y

. Thus, the periodicdomainstructure is stablenear the patterned wall, but further away

the domain patterncoarsens.

Such a behavior, i.e. a rapid formation of a patterned equilibrium structure in thin lms,

but alateral domaincoarsening afterwards inthick lms, has alsobeen observed innumerical

treatmentsoftheCahn{Hilliardequationwithappropriateboundaryconditions[Kar98,Kie99]

and in experiments [Kar98]. Moreover the equilibrium structures that have been found in

ref. [Roc99], i.e. large scale phase separation far away from a nanoscopically patterned wall,

but a remainingstructure near the wall, cf. sec. 1.4, agree with the present results.

In both cases considered so far the periodicity L

k

was comparable to or larger than the

bulk demixing length

m

. The question arises of what happens for L

k

m

. In this case,

we expect that the patternedsurface induces structures,which are toosmalltodrive spinodal

decomposition because the interfacial energy of such structures is higher than the free energy

gained by decomposition.

To investigatethe interplay between the twolength scales L

k

and

m

we consider aslab of

thickness L

z

= 12:5 and vary L

k

. We note that strictly speaking,

k;m

is the relevant length

scale for lateral decomposition in a slab. However, for L

z

=12:5 the demixing length

k;m is

close tothe bulkvalue

m

,cf. sec. 6.3.3.

Figure 6.15shows corresponding lateralstructure factors I

y (k

y

;z;t)for t =1000 MCS and

forL

k

=6;12:5;and25. Inthe caseofL

k

=6

m

,g.6.15a,the peakscorrespondingtothe

surface induced structure and the lateral modes are comparable. The demixing process is not

dominated by the surface{induced pattern. Also, the induced structure develops much more

slowly compared to the case of L

k

= 12:5 '

m

, shown in g. 6.15b. In this case, the peak

corresponding tothe ordered structureis afactor ofabout 10higher,and the lateraldemixing

modes arethusalmostinvisible. ForL

k

=25

m

adoublepeakstructureemerges. This can

be interpreted in terms of a pattern directed spinodal decomposition wave, i.e. if one looked

at the concentration uctuations Æc

A

(y) = % 0

A

(y) c

A

in the yz{plane and labeled positive

and negativeregionsofÆc

A

(y) blackand whiterespectively, onewould see acheckerboard{like

pattern [Kie99].

Tosee moredirectlyhowinthelastcasesuchapatternpropagatesintothelm, weplotted

in g. 6.16 the intermediate scattering function I

y (2=L

k

;z;t) as a function of z for various

timestforasystemwithL

z

=25andL

k

=50. Thispicturedescribeshowthe surface{induced

periodicdomain patterns grow in perpendicular direction. Since our lmthickness is limited,

we did not tryto quantify the propagationof this kind of kinetics further. Forvery large lm

thicknesses wewould expectthe usualLifshitz{Slyozovdomaingrowthtooccuratlargetimes.

In this work we described long{time kinetic properties of polymeric systems. Particularly

we considered the case of a binary polymer blend conned between two walls that could be

homogeneousor heterogeneous.

Since the long{time kinetics can hardly be reached within models that resolve the chain

structure of the polymers, coarse{grained models have to be used. We employed two kindsof

treatments: First,weusedadescriptionbasedontimedependentGinzburg{Landautheory,i.e.

onthe Cahn{Hilliardequation(CHE)thatdescribesthe kineticsofthe systemsviaanonlinear

partial dierential equation for the order parameter eld. Secondly, we treated the systems

in the framework of soft particle models. In this case one polymer is mapped onto one soft

particlewithinternaldegrees offreedom. Thechainstructure isnot resolved, butthe polymer

is modeled by a monomer density for a given state { or shape { of the chain. The kinetics of

the system is suppliedby adiscrete time MonteCarlo algorithm.

AgoodphenomenologicaldescriptionofphaseseparationprocessesisgivenbytheCHEthat

inthe case ofconnements issuppliedby appropriateboundary conditions. From the analytic

solution of the linearized problemthat is valid for short times, a criterion for the suppression

ofsurface directed spinodaldecompositioninthin lmscouldbe derived. Accordingtothis no

SDWoccurs if thelmthickness issmallerthan halfthe criticalwavelength, L<L

crit

==k

c .

A numerical solution of the CHE is complicated by the fact, that the corresponding line

system is sti. This strongly restrictsthe size of the possible time{steps for explicit methods

in order to avoid numerical instabilities. This problem was solved by applying an implicit

time{steppingscheme that allows toexplore the whole kinetics ofphase separation until

equi-librium. The eÆciency of the method is particularly of importanceconsidering the new time

scales arisinginconned systems. Especiallythe perioddoublingprocess occurringin thelate

stages of quasi one dimensional phase separation could be explored. However, the implicit

method involves the inversion of huge matrices inthe solution of coupled nonlinear equations

by Newton's method and therefore isat the moment practicablyintwo dimensions only.

Therefore soft particle models have been developed, based on ideas by Murat and

Kre-mer[Mur98 ]. Herebythefreeenergyfunctionalofthesystemisdecomposedintoan

intramolec-ular and an intermolecular part, the rst being determined by the probability for the internal

states of the particle, the second by the intermolecular interaction energy of the monomer

densities. However, instead of using self{avoiding chains as an input, as in ref. [Mur98], in

the present work Gaussian chains providethe underlyingchain model. The self{interactionof

the chains, i.e.interactionof dierent monomersof one polymer,is treatedconsistentlyonthe

same footingas the interaction of monomers belongingtodierent polymers.

The main advantage of this approachis that the model nowfullls the basic scalingrelations

of polymer systems without the necessity toadjust the interaction parameter as a function of

chain length. Particularly, no simulations of explicit chains are therefore needed in the setup

of the model. Further on, for Gaussian chains the monomer densities can be approximately

described by simplefunctions,allowingforaneÆcientanalyticalcalculationofthe overlapand

making the model highlyportable.

Whiletheinputquantitiesaregivenforsomepossiblesoftparticlemodels,i.e.fora

descrip-tion as spheres, ellipsoids and dispheres, the simulationswere done for the Gaussian ellipsoid

model(GEM). Within the GEM ithas been shown that not only many features characteristic

for polymeric systems can be found, for example, the correlation hole in a homogeneous melt

or the orientation and deformation of the particles' conformations at phase boundaries, but

moreover the model is very eÆcient, such that the late stages of phase separation processes

can bereached.

Finally, conned systems were studied with the GEM. For a binary blend conned

be-tween two homogeneous neutralwallsan increase of the lateral demixing length

k;m

and the

corresponding demixing times with decreasing slab thickness was found for L

z

<

m

. This

supports the results based onthe CHE, but now in a more realistic model, and suggests that

experimentalstudies of this eect shouldbe promising.

The case, where one of the two walls is structured, corresponds to experiments that try

to transfer the pattern of the substrate on the domain pattern. Two dierent equilibrium

patterns are found. Either the structure propagates through the whole lm, leading to a

striped demixingpattern(\fullstructure"), orthesurface induced structureoccurs onlyinthe

vicinity of the wall(\partialstructure"). Which patternemerges, depends on the ratio L

z

=L

k

only. This is explainedby a considerationof the involved surface energies.

Dierent equilibrium patterns lead to dierent kinetic pathways for spinodal

decomposi-tion insuch a lm. In the case of anequilibrium patternwith full structure, pattern directed

spinodal decomposition is the dominant process. The periodic ordered pattern freezes after

reaching the opposite wall. On the other hand, the penetration depth of the pattern directed

spinodal wave remains nite and lateral domain coarsening takes place in the late stages of

decomposition. In the case of small pattern periodicity (L

k

<

m

), pattern directed spinodal

decompositionis less pronounced, asthepatterninducesunfavorable structureswith toolarge

interfaces.

Insummary, weshowed that thekindof softparticlemodels developedinthis work supply

a useful and very eÆcient tool, to study polymer systems on large time and length scales.

While a direct connection between soft particles and Gaussian chains exists, no simulations

of systems of chain models are needed in the implementation. The models are especiallywell

suited, tostudy phase separation processes.

Therearemany applicationsthatcan bethoughtof. Firstofall,itshouldbeinterestingto

study diblock copolymers with the disphere model. In such systems it is diÆcult to simulate

even the phase diagram with chain models, because a possible incommensurability between

the periodicity of the microphase separated structure and the system size can lead to strong

nite size eects [Bin94, Bin99]. Therefore large systems are needed in the simulations that

can be provided by soft particle models. The inuence of the morphology on the long{time

still poorly understood froma theoretical point of view. In this respect simulations based on

the disphere modelmay help toidentify the underlying processes.

From amore conceptualpointof view, itisimportanttoexamine thehierarchy ofpossible

multisphere models that havebeen proposed in sec. 3.6. This would not only leadto adeeper

understanding of the second coarsening step, but provide a more direct connection to chain

models and make a remapping, i.e. a substitution of soft particles by chain molecules, easier.

Moreover, it could be thought of basing a thermalizationprocedure for explicit chain models

on this hierarchy. Large scale structures could hereby be thermalized on a very coarse scale,

while smallscale structures could be treatedon aner scale.

Here wegive the discretization of the Cahn{Hilliard equation (2.23) and the boundary

condi-tions eqs. (2.26a,b) and their static version eqs. (2.28a,b). Since the CHE(2.23a) is validalso

atthe boundary, eqs. (2.26a,b) are rewritten by

@

for all times t. In this section we suppress the time argument wherever it is convenient.

Denotingthenumberofgrid pointsbyN

x

1)in slab geometry. The space grid is

dened by

the set of interiorgrid pointsis dened by

and the set of boundary grid points isgiven by

Æ

Forthe grid functionswe use the notation

i;j

(t):=(ix;jy;t);

i;j

(t):=(ix;jy;t): (A.5)

To deduce an appropriate semi{discrete model for the underlying continuous problem, the

spatial derivatives of somefunction f =f(x;y)are replaced by standard symmetricdierence

formulae of order 2. In terms of the discrete f

i;j

Here we dened := x=y. The discrete versions of the continuous eqs. (2.23) yield a

N

x N

y

dimensional system of coupledordinary dierentialequations

@

). In the determination of @

t

, virtual variables occur, corresponding to grid points that are not in

x;y

. These

virtual variableshave tobereplaced by the boundaryconditions. In the bulkcase the virtual

variablesin eq.(A.8a) can bereplaced by the discrete periodicboundaryconditions

In the caseof aslab eq. (A.10)is replacedby thediscretizationof the no{ux condition(2.25)

Note, that the splittingof the originalCHEinto twoequations withan explicitrepresentation

of leads to a convenient use of the no{ux condition to eliminatethe virtual variables. To

determine the virtual variablesin eq. (A.8b), we discretize the second boundary condition. In

the bulkcase this leads to

In the case of a slab, we have to discretize eqs. (A.1a,b). We start with the lower boundary

(y =0)and obtain

Solving this equation for

i; 1

and using eq. (A.11) yields

Note, that by periodicity

1;0

. Inserting eq. (A.15) in eq. (A.8b)

for j =0 yields

i;0

with the matrix

A I+

where I denotes the identity matrix. The inhomogeneity is given by

An analogous calculation forthe upper boundary (y =N

y

1)yields

A

SinceAispositivedenite,eqs.(A.17,A.20)haveauniquesolutionforevery ;xand

s

>0.

Theinverse matrix A 1

can bedeterminedbeforetime integration by Choleski{decomposition

LL

In the case of quasi{staticboundary conditions (eqs. (2.28a,b) corresponding to

s

!1), no

system of equations has to be solved (A = I). Thus

j;0

vanish ineqs. (A.19, A.21).

To summarize, the problem to be solved numerically consists of the ordinary dierential

equation (A.8a), together with the replacements (A.9, A.10) for the chemical potential in

the bulk case and (A.9, A.11) in the slab case. The variables for the chemical potential

i;j

themselvesare given ineq.(A.8b) withthe replacements(A.12, A.13) inthebulkcase andthe

special representations of

i;0

and

i;N

y 1

given by eqs.(A.17, A.20) inthe slabsituation. The

system of dierentialequations iscompleted by the initialvalue condition

i;j

(0) =(ix;jy;0): (A.23)

B.1 Averages of Gaussian Chains

HerewepresentmomentsoftheeigenvaluesSasobtainedbyMonteCarlosimulation. TableB.1

displays results for chains of length N = 1000 averaged over 10 7

dierent realizations. The

data for the radius of gyration R

G

are given for the sake of comparison. The deviations from

the exact values for N !1 are due tostatisticalerrors and nite chain lengths.

Table B.1: Moments ofthe eigenvaluesS asdetermined byMonteCarlo simulation.

hR 2

G

i=N 0.16685 hR 4

i=N 0.12758 hS

2

i=N 0.028708 hS 2

i=N 0.010568 hS 2

0.0038714 hS 3

0.00032239 hS 3

2 i=N

3

4:620610 5

0.0013717 hS 3

3 i=N

3

1:933810 6

B.2 Parameters of the Distribution Functions

The determination of the parameters of P

R

momentsoftheheuristicfunctionsarecalculableanalytically. Thereforewedenetheconstants

a

i are exact

in the limit N ! 1. With this denition and the well known results hR 2

=540, cf. [Yam71],we are led tothe two equations

a

At this point we also give a more quantitative test of P

R (R

2

G

) by comparison of the higher

momentsofR 2

G

. The asymptoticexact resultforthethirdmomentishR 6

G i=N

3

=631=68040

0:009274,whilewendhR 6

G i=N

3

=0:009280. ForthefourthmomenttheexactresulthR 8

G i=N

4

=

1219=4082400:002986 has tobecompared with hR 8

G i=N

4

=0:003000.

For P

(S

)the same procedure leads to

hS

SincenoexactanalyticalresultforthemomentshS m

iexists toour knowledge,thesequantities

aredeterminedbyMonteCarlosimulationsofGaussianchainsoflengthN =1000. Theresults

are given in tab. B.1.

B.3 Improved Formula for the Monomer Density

For the sake of completeness, we present animproved heuristic formula for the density of the

x

A least squares tof the constants yieldsu

2

=0:674 and 0

2

=0:748.

B.4 Improved Calculation of P

C

Here, we present an improved approximation for P

C

). On this behalf, we make

the ansatz

P

whichisinspiredbythecumulantexpansion. ThecoeÆcients 2

aretobedetermined

by the conditional momentsdened ineq. 4.26.

It is possible, to determine approximatively higher moments than the second one from

eq. (4.19),

In the determinationof the fourth and sixth momentsome integralsare neglected, that could

not be solved exactly. We checked the accuracy of the expressions (B.5,B.6) by Monte Carlo

simulations and found a satisfying agreement, the relativeerror being smaller than about 0:1

in the regions of high probabilityP(R 2

A

;R 2

B

),justifying the result a posteriori.

ThenthecoeÆcients 2

aregiven intermsofthe conditionalmoments(4.27,B.5,

B.6). Astobeexpectedforthiskindoftreatment(acutocumulantexpansion),thepolynomial

term is negative for large u

AB

and thus also P

C

. This failure can be compensated

by increasing the degree of the polynomial by one and requiring, that this polynomial has a

minimum,wherethe originalpolynomialgoestozero,thusdeterminingthe coeÆcienta

3 . The

B.4 Improved Calculation of P

C (r

AB

;R

A

;R

B )

spurious error for large u

AB

can be minimizedby dividing the polynomial by a suitable term,

leadingto

P

C (r

2

AB

;R 2

A

;R 2

B )=C

r

r 2

AB

2

3

2

0

3

2

exp

3

2 u

AB

1+a

1 u

AB +a

2 u

2

AB +a

3 u

3

AB

1+a

3 u

3

AB

: (B.7)

AswearemainlyinterestedindeterminingF

intra

,thedeterminationofthenormalizationfactor

C is of minor importance, because it leads to an additive constant only. (If necessary, it can

be determined eithernumerically orin terms of amodied hypergeometricfunction.)

In principle, a systematic polynomialexpansion of this kind is possible, the coeÆcients a

i

being determined by higher conditional moments.

C.1 Ellipsoid{Ellipsoid Interaction

Inthissectionwederiveanexplicitexpressionfortheinteractionbetweentwoellipsoids,dened

ineq. (3.5) in the case that the monomer densities are given by eq. (3.17).

When inserting eqs. (3.17, 3.16) into eqs. (3.13, 3.5) the calculation of F

inter

reduces to a

sum of nine terms of the form

Z

where the functions (j)

were dened ineq.(3.17) andspecied intab.3.2. Moreover, w (j)

dependingonwhichof thethree termsineq. (3.17a)contributesto (j)

(y ). With

the denitions

expression (C.1) reads

1

it follows that

The quadratic form(C.6) can berewritten as

T(y)=

which yields

Z

C.2 Ellipsoid{Wall Interaction

The integrals in eq. (6.2) with a potential of the form eq. (6.3) and monomer densities, that

are essentially sums and products of Gaussian functions, see eq. (3.17), can be cast into the

more general form already treated in the previous section C.1. The six resulting integrals of

eq. (6.2) are of the form