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High Pressure Experiments in Soft Condensed Matter

G.Meier

1

, H. Kriegs

1

, P. Lettinga

1

, J. Kohlbrecher

2

1

Forschungszentrum Jülich ICS-3, D-52428 Jülich

2

Paul Scherrer Institut, CH-5232 Villigen

Pressure range:

1 bar < P < 5000 bar Optical transparent:

for DLS/DWS Temperature range:

0°C < T < 80°C Sample volume:

10 mm x 2 mm Pressure jumps:

P up to 1500 bar and faster than t < 0.5s

for cyclic experiments

5000bar pressure cell for combined SANS-DLS/DWS

2000bar pressure cell for DLS with conservation of polarization plane

Pressure range:

1 bar < P < 2000 bar Conservation of polarization plane:

for VV and VH experiments Temperature range:

-20°C < T < 150°C Sample volume:

round cell, 2cm3 Different angles:

At the same time PCS and FPI:

Frequency range [Hz] 10-2-107, 109-1011

1000bar pressure cell for microscopy including confocal imaging

Pressure range:

1 bar < P < 1000 bar Temperature range:

10°C < T < 80°C Confocal image (FCS)

Use of diamond window and small sample volume 1μl, otherwise pill 500μl

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