I N ~ T I T ~ T E OF PI~YSICS PUBLISHTYG S U P E R C ~ N D U ~ R SCIENCE AND TLCHNI)LIIGY
Supercond. Sci Twhnol. I 8 (2005) 385-187 doi- 10.1088M953-2W8II RI1W2
Velocity measurements of the dendritic instability in YNi2B2C
R Biehler" B-U Rungel, S C ~ i r n b u s h * . ~ , B Holzapfe12 and P Leiderer "
I Depanmcnt of Physics, Univcnrly or Konstan~, Universitatssuafle 10.78464 Konstanz, Germany
? IFW Dresden. PO Box 2700 16.0 1 17 1 Dresrlen, Germany E-mail: Bjoem.Bichler@uni-konstanz.de
Rcccived 19 July
2004,
in finalform 8 November
2004Published
1February 2005
Online
atstacks.iop.org/SUST/18/385
AbstractWc measured the
velocityof
Ihcflux front of an artificially
nucleated dendritic instability inYNi2B2C.
Therequired
t i m e resolutionIn
the nanosecondregime was
achievedby our
magneto-optic pumpprobetechnique,
utilizinga
f e m t o s e c o n dlaser
system.The
penetration vclocity ofthe flux
frontis
on the orderof 360 km
s - ' .(Some
figurcs in
thisarticle are in
colouronIy
in theelectronic version)
1. Introduction
The dendritic ~ n s t a h ~ l i t y is a rapid redistr~bution of magnetic flux inside a type
E
supercunductor (e.g. see [I]) and was found in 1967 by Wertheimer er a /[2];
in YNi2B2C it was first observed by Wimbush e# a1 [ 3 ] . The instability can be tripgemd aflificially by disturbing the screening current distribution inside the wperconductor. Thls can be caused by sweeping the magnetic field 141. hy applying a transport current [S] or by heatrng a small ponion of thc s u ~ ~ ' c o n d u c t o l : The latter was used to determine the flux front velocity i n YBCO, which was found to be on the order of 160 km s-' [6].Despite the efforts made to undcrstantl the details behind the instability mechanism they rcmain unknown. This is the reason why we want to put forward additional data
on
the dynamic behaviour of the dendritic instablli ty in YNi2B2C.2. Sample preparation
Fur this work.
a
thln film of YNi2B2C was deposited in an ultrah~gh vaccuum (base presqure < 10-' mbar) pulsed laser deposition system, as descr~bed In [7]. A polycrystalline YNi2B2C target of stoichiometric cornpositron, prcpared by arc melt~ng, was lired upon at 30 Hz with an energy density a5 J cm-', leading to a depobition riite of around 2 nm s-' on the MgQ(001) substrate, polished on both'
Present addrew Yational Institute for Matenal~ Science. InternationalCenter for Young Scientists. 1-1 Nam~hi. Tsukuba, lharak~ 305-0044. Japan
t
YNlzBzC magneto-oplic film wfth layer cameravanaMe delay line
Figure 1. For time resolved picrures we use a pumpprobe techn~quc The laser pulse is used to trigger the instability and some nanosecond^ later for illumination. For non-time-resolved images a cold light source can be used for illumination. For clarity the lenses of the pularizmg microscope (right part) arc not shown.
iides, held around 2 cm abovc the target. The deposition temperature was 750°C. and the film thickness was around 350 nm Structural analysis of the film was performed using x-ray 8-26! measurements followed by in-planc texture dctcrminatinn (pale figure measurement). 8-28 and pole figure x-ray characterization indicate c-axih oriented epitaxial f l m growth with the dornlnant orientation rotated by 45" in plane with respect to the substrate: YNiZB2C(OOi)[l 101
11
MgO(001)[100]. Thc svperconducting transition temperature, T,, was measured inductively using an alternating magnetic field shielding technique. yielding
a
Tc of12
K witha
transition width of 1.5 K.0953-20jR/05/040385+03$30 00 O 2005 10P Publishing Ltd Printed In the UK 385 First publ. in: Superconductor Science and Technology 18 (2005), 4, pp. 385-387
Konstanzer Online-Publikations-System (KOPS) URL: http://www.ub.uni-konstanz.de/kops/volltexte/2007/2728/
URN: http://nbn-resolving.de/urn:nbn:de:bsz:352-opus-27281
R Biehler er a1
Figure 2. Magneto-opt~cal i~liages uC the flux d~stl.~butiortin YNi?B?C:: (a) initinl condii~on, (b) afrer 3 9 ns, and ( c ) -10 s (the final state).
T h e cxternnl field was B,, = 1.32 m T at 4 h K For clarity a plane was subtracted from the initinl image (a) and the contrast enhanced.
(h) and (c) were rercaled according to equsuon ( 1 ) The firs1 arrow ( 1 ) In part (b) marks the minimum penematton length and the second arrow (2) marks the maximum cornparible wfrh the measurement. The w h m line on the right of each picture indicates the sample edge.
Note that the front of the final state (c) 1s much clearer (ind~catcd by n m w ( 3 ) ) . The length scale remains the same in each panel.
3. Experimental set-up
A sketch of the experimental set-up 1s hewn in figure 1 We apply a p u m p p r o b e tcchiiique usrrlg ;i conimercial femtosecond laser system. It produces pulscs of VWHM =
150 fs at b = 800 nm. We split the beam in two parts; one is used to perturb thc current distr~butlon by Iwally heating the superconductor. Under appropriate cclnrlitionu [XI this w ~ l l triggel. the instability. T h e second pan of the pulse i s fed into a delay line which has been adjusted for time delays betwccn 1 aiid 6.5 ns. After passing through a polarizer t o ensure a well polarized beam, the light i~ used to take a rnagncto- optical image of the instantaneous flux distribution. This is done by an iron garnet film showing
a
large Faraday cffect, i.e. the polarization of light i s rotated proportionally to the local perpendicular mapnctic field compnnent. Thir givesa
snapshotof
the flux distribution just above the sample. We focused the pump beurn at the sample cdge. h r away from the comers. Asa
camera we usc a 12-bit slow scat1 CCD camera w h l c l ~ was coilled to -40 'C. Rcsults c ~ f a slrnilar experiment with YBCO thin filmsare
published i n [6j.4,
Results and discussion
A typical expcrirnent was conductcd as followh. The sarnpIc was zem-field cooled to a ternperatrtre of T = 4.6 K and an external magnetic field 1.3 mT
<
R,,,6
5 . 2 mT wayapplied. Then the pump-prohe run was conducted and after
~ 1 0 s an additional picture of thc final qcare was taken. Wc measured the energy El,,,, of each lascr pulse and scaled
the intensity of the images by this factor. In addition we apphed a divisionldifference technique to improve the s~gnal- to-noiw ratio and reduce the effects of interference and uneven illumination. This was done by measuring the flux distribution:
twice before ( I I , 12) and once during the p u m p p r o b e run
(4).
The final images
as
seen in figures 2(b) and(c) were constructed by the fol!owing calcufat~on:whcre El,,,,>, is the energy of thc h e r pulse with whlch the nth image was taken. The division of two pictures should be read
as
dtvtding the images pixel by pixel. Note that this will lead to nn image emphasis~ng the changes of the flux distribution. Note that this procedure cannot be applied for the initial condition (figure 2(a)), since the subtraction would result i n a uniformly black image.Repeating thip experiment for different external fields and variuus delay times gives snapshots of the momentary flux disirihutinn. We measured the distance
from
the sample edge ro the Rux front; this is plotted in figure 3. The error bars lndicatc the maximum and minimum distance consistent with the magneto-optical images. The dotted line in figure 3 corresponds to a velocity of a360 km s-'. This is much faster than the velocities measured in YBCO. There we werc ablc fo distinguish two well separated velocities: an early strtge showing a dependence on the external field(i.e, a
high field Ied to a high velocity of u p to 160krn
s-I), and a decrease in velocityto
18 km s-' at times larger than 10 ns, Largely independent of theexternal
field and temperature.Velocity measurements ofthe dendritic instability in Y N i z B z C
Figure 3. Flux penetmtron length as a runchon o f (a) lime and (b) exte~,nally appl~ed field. The doned tine is a guide to the eye corresponding to a velocity of -360 k111 s - ' Note the decrease in velocity f o r tlrneq 3 4 ns.
These wel! defined stages were not seen in YNi2B2C. A possible explanation may be that rhe low velocrty of the flux front In YBCO was observed as the dendrite penetrated into the Meissner phase region of the sample. In the case of YNi2B2C the Shubnikov phase extended over a region of z 1 . 2 mm, which 1s approx~~nately the total length of the
dendrites investigated. Therefore we would expect the veloc~ty to decrease as soon as the dendrite enters the Melssner region.
Acknowledgments
We are grateful for the sponsorship by the Gerrnnfi Isrneli Foun- dation. The work in Dresden was supported by the Deutschc Forschungsgemeinschaft as par? of SFTI 463 'Rare earth tran- sition metal compounds: stnlcture, magnetism and transpon'.
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