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Future Facilities for In-situ Observation of Solidification Processes

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A LUDWIG’“ J MOGERITSCH” (on behalf o l the METCOMP team)

'European Space Agency— ESTEC (NL). :NTNU (NO), 'ACCESS e.V. (D). JL2MP(F). 'Kalholieke Universiletl Leuven (B). °DLR Cologne (D).

'University College Dublin (IRL), *TU Beilin (D), ‘“INSP (F), ,0Montanun~iversitaet Leoben (A)

Ongoing reorganisation of a hexagonal directional- solidification pattern of a transparent eutectic alloy (succinonitrile-d,camphor) Oblique view in dark filed (the eutectic crystal phase that forms fibers is lit) Growth di­

rection upward

Sequence of images ot refined Al-3 5vrt%Ni solidification, recorded during the CET induced by a sharp pulling rate jump (1,5 to 15pm/$) by synchrotron X-ray radiography. The solid mainly constituted of aluminium appears in grey while Ni enriched liquid is dark.

Columnar dentritic and planar eutectic growth in AI-30CU (G=27K/mm. v=-22.5pnVs)

‘Formation of eutectic cells in thin, polycrystalline sam­

ples from ternary organic SC hi-DC- NPG alloys'1. In the presence ol a third alloying element (NPG) me eutectic solid / liquid interface, composed of SCN and DC grow­

ing from the liquid, is constitutionally supercooled and subject to a complex sequenoe of instabilities that lead to cell form aboil.

SCN: SUDCNUnlrU, DC OCrtmptttr, MPG:NtfCfjßrrt(1fll^cl

"Columnar-Equiaxed-Transition in Neopentytglycol- Camphor1’. In the figure you see the columnar front, me first occurrence ol equiaxed dendrites and on me left-pad the front of a solid-state transformation.

Court my: L2MP. ACCESS

Planar eutectic solidification growth AI-30Cu (G=46K/mm, v=6 4umfs)

Point of Contact at the European Space Agency:

Dr. Olivier Minster Head of Physical Science Unit Olivier. Minsier@esa.int

Dr. Daniela Voss Materials Science Coordinator Daniela Voss@esa int

Dr. Peter Behrmann DIRSOL Technical Officer Peter.Behrmann@esa.int

Future Facilities for

In-Situ Observation of Solidification Processes

D. VOSS1. B BEHRMANN’ . R. LINDNER’ . S. VINCENT-BONNIEU1, O MINSTER , D, JARVIS1;

R. MATHIESEN2, P. SCHAFFER2. G. ZIMMERMANN3. H NGUYEN-THI FROYEN5, M. KOLBE5, D. BROWNE , F GARCIA-MORENO0, (on behalf Of the XRMON team) S. REX (on behalf of the SETA team),

L. STURZ , G. FAIVRE\ S. BOTTIN-ROUSSEAU9, S. AKA MATSU , M. PERRUT9 , N. MANGELINCK ,(on behalf of the CETSOL and SEBAteam)

Introduction:

within the ELIPS (European Programme for Life and Physical Science) Programme of the European Space Agency two facilities are currently planned to support in-situ observation of solidification processes; DIRSOL and XRMON.

Directional Solidification Facility (DIRSOL) X-Ray Monitoring of Advanced Metallurgical Processes (XRMON)

Directional Solidification Experiments of Bridgman Type with

transparent alloy model substances Directional Solidification Experiments of Bridgman type of Diagnostics by optical observation at high resolution metallic alloys

monitoring by state-of-the-art in-situ X-ray radiography S cien tific O bjectives:

to study and gain deeper understanding of Scientific Objectives:

the pattern formation and instabilities during To study and gain deeper understanding of solidification of multiphase alloys along a eutectic path - columnar to Equiaxed dendritic growth the columnar to Equiaxed transition (CET) morphological instabilities of ternary alloys

peritectic reactions - particle pushing at cellular and dendritic interfaces in

metal matrix composites unconstrained growth macrosegregation of Al-based samples

lies (ram ternary organic SCN-DC-

rrzs

200um

Accommodation; to be planned as a frequent flyer on up Accommodation; in MSG (Microgravity Science Glovebox) on coming parabolic flights and sounding rocket missions

board the ISS Launch in spring 2009

In Phase B (readiness for launch 2010)

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