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Agroscope, Competence Division, Plants and Plant Products | 2018

The Golden Spirit

an analytical-based approach to improve sensory quality of spirits Sonia Petignat-Keller1, Martin Heiri1, André Marti2, Sharona Perrin2, Jonas Inderbitzin1

1 Agroscope CH-8820 Wädenswil, 2 METAS CH-3003 Bern-Wabern

Conclusion

The detailed study and comprehensive data collection over six years provide an overview on thediversityof Swiss spirits. Our mission is to support distillers in the development and promotion of outstanding products through knowledge transfer. Decision tree models for predicting expert evaluations help to improve the quality of certain product categories and thus increase product acceptance.

Methods

GC-FID, GC-MS and HPLC for analysis and individual ratings by expert judges according to a 100-point system for appearance, odor quality, odor intensity, taste quality, taste intensity, mouthfeel and harmony/complexity were used. Instrumental data included alcoholic strength by volume, extract, methanol, higher alcohols (fusel oils), ethyl- carbamate, sugar, thujone and several volatiles. Instrumental analysis of all submitted products were carried out underaccredited conditions(ISO 17025).

Results

Out of 38 parameters three showed to influence the judgement of apple spirits significantly. Ethyl acetate ≥ 395.5mg/LrA (main head compound) and

2-butanol < 46 mg/LrA (tail compound) had a negative effect, whilediethylsuccinate > 6mg/LrA appeared to have a positive effect on the overall assessment, possibly due to increased fruitiness and typicity (Fig.2).

Introduction

DistiSuisse is an associationpromoting the quality of Swiss spirits. Their nationalproduct awardis the largest in Switzerland, taking place every two years. It helps to preserve a Swiss cultural heritage and to promote its status in our society. The aim of the study was to gain understanding of analytical parameters and their effects on sensory quality, as rated by expert judges. Based on the last three events, 1424 spirits out of 19 categories were analyzed.Decision tree modelsto predict expert ratings are proposed for specific product categories. Observed cutoff points for analytical parameters and sensory quality are shown by usingapple distillates as an illustration, since this was one of the least good judged category beside apricot and williams (Fig.1).

Fig. 1: Expert ratings for different categories of spirits at the DistiSuisse awards 2013-2017.

Fig. 2: Decision tree for the expert ratings of apple spirits.

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