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1.) Load sample into Prepchamber How to load a sample using the ELMITEC load lock for transfer into the PEEM.

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(1)

PEEM load-lock Manual

07.06.2005

I:\manuals\Load_LockManual2.doc - 1/2 -

1.) Load sample into Prepchamber

How to load a sample using the ELMITEC load lock for transfer into the PEEM.

Location

• The load lock is located below the prepchamber on the left-hand side of the PEEM.

• The forevacuum buffer is in the rack WSLA 13.0.55

1.1.) Venting the load-lock

Venting the load-lock to insert the new sample.

o Turn N2 gas ON (behind hutch) and check for flow.

o Set Buffer controller to P2 = ACTIVE.

o Check that valve separating load-lock / prepchamber and prepchamber / mainchamber are CLOSED.

o Turn TMP controller (DCU) Power = OFF o Wait until load-lock is vented.

Vent valve opens once speed is below 1350/min, after ~3 min.

Buffer controller

TMP power Buffer1

pressure

Buffer2 pressure

Load- lock

2 Screws

(2)

PEEM load-lock Manual

07.06.2005

I:\manuals\Load_LockManual2.doc - 2/2 - o Open CF40 flange

o Turn N2 gas OFF (behind hutch).

1.2.) Install new sample

Install new sample and prepare for pump-down.

o Close CF40 flange (two M6 screws and VITON gasket).

o Set Buffer controller to P1 + P2 = ACTIVE.

Wait 50sec until valve opens (Vent 1 lights up).

o Turn TMP controller (DCU) Power = ON

Check that pressure goes down (10-2 mbar after ~ 1min).

o When PLOAD < 2 10-6mbar transfer sample.

Known problems:

¾ Sometimes the vent valve of the TMP does not close. Turn TMP controller OFF / ON

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